Sodium Hydroxide → 4-(3,4-Dimethoxybenzoyl)benzoic acid

HRID 2414434노트

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HRID 2414434 반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:18]=[CH:19][C:20]=1[O:21][CH3:22])[C:6]([C:8]1[CH:17]=[CH:16][C:11]([C:12]([O:14]C)=[O:13])=[CH:10][CH:9]=1)=[O:7].[OH-].[Na+]>C(O)C>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:18]=[CH:19][C:20]=1[O:21][CH3:22])[C:6]([C:8]1[CH:17]=[CH:16][C:11]([C:12]([OH:14])=[O:13])=[CH:10][CH:9]=1)=[O:7]

참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 22645197Methyl 4-(3,4-dimethoxybenzoyl)benzoate

생성물 1

HCID 226452014-(3,4-Dimethoxybenzoyl)benzoic acid

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

1.3 g (4.33 mmol) of methyl 4-(3,4-dimethoxybenzoyl)benzoate was dissolved in 50 ml of ethanol. 7 ml of 1 N sodium hydroxide solution was added to the obtained solution, and they were stirred overnight. The solvent was evaporated, and the residue was washed with ethyl acetate and then filtered to obtain the title compound.

후처리

  1. customThe solvent was evaporated
  2. washthe residue was washed with ethyl acetate
  3. filtrationfiltered

출처 및 근거

ORD 기록
ord-53d65ee6a16f42aca430a61635896b25
출처 데이터셋
uspto-grants-2004_11
특허 번호
US06812231B2

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