Triethylamine → HCID 136347703, 화합물
반응식
[C:1]([C:3]1[C:4](=[O:10])[NH:5][C:6](=[O:9])[NH:7][CH:8]=1)#[N:2].Cl.[NH2:12][OH:13].C(N(CC)CC)C>CO>[OH:13][N:12]=[C:1]([C:3]1[C:4](=[O:10])[NH:5][C:6](=[O:9])[NH:7][CH:8]=1)[NH2:2]참가 물질
5
실험 절차
5-Cyano uracil (2.0 g, 14.6 mmol) was suspended in methanol (50 mL), then hydroxylamine hydrochloride (1.4 g, 20.0 mmol) and triethylamine (2.8 mL, 20.0 mmol) were added and the mixture was heated to reflux overnight. The mixture was cooled to room temperature, the solid was collected by filtration, washed with methanol and dried to give the title compound as a pale yellow solid (1.8 g).
후처리
- temperaturethe mixture was heated
- temperatureto reflux overnight
- filtrationthe solid was collected by filtration
- washwashed with methanol
- customdried
출처 및 근거
- ORD 기록
- ord-847b5d1e0bfe4579a03ca873d9a9f2b9
- 출처 데이터셋
- uspto-grants-2004_11
- 특허 번호
- US06821972B2
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