Hydrochloric Acid → 2-Methyl-1-phenylpiperaZine hydrochloride

HRID 2416657노트

반응식

HRID 2416657 반응식
[CH3:1][CH:2]1[N:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH2:6][CH2:5][N:4](C(OC(C)(C)C)=O)[CH2:3]1.[ClH:21]>C(OCC)(=O)C>[ClH:21].[C:8]1([N:7]2[CH2:6][CH2:5][NH:4][CH2:3][CH:2]2[CH3:1])[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 226330714-Boc-2-methyl-1-phenylpiperazine

생성물 1

HCID 226330592-Methyl-1-phenylpiperaZine hydrochloride

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

(±)-tert-Butyl 3-methyl-4-phenylpiperazine-1-carboxylate (142 mg) was dissolved in 4N hydrogen chloride in ethyl acetate (5 ml). After stirring for 15 minutes, the solvent was removed under reduced pressure to give the title compound as a slightly yellow solid.

후처리

  1. customthe solvent was removed under reduced pressure

출처 및 근거

ORD 기록
ord-bad87fa887ec45f383499b68be82f86c
출처 데이터셋
uspto-grants-2004_11
특허 번호
US06825200B1

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