Hydrochloric Acid → 2-Hydroxydodecanoic acid

HRID 2417574

반응식

HRID 2417574 반응식
Cl[CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[C:3]([OH:5])=[O:4].[OH-:16].[K+].Cl>O>[OH:16][CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[C:3]([OH:5])=[O:4]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 14797Potassium HydroxideHCID 43873702-chlorododecanoic Acid

생성물 1

HCID 977832-Hydroxydodecanoic acid

시약·촉매·용매 1

HCID 962Water용매

실험 절차

0.1 Mole of alpha-chlorolauric acid prepared in the foregoing manner was admixed with 500 mls. water and 0.4 moles of KOH in a suitable reaction vessel and stirred overnight at a temperature of 98°-100° C. The reaction mixture was poured into a separatory funnel, to which was added hydrochloric acid (40 ml. conc. HCl in 200 ml. H2O). The mixture was extracted with chloroform. The chloroform layer was removed and the CHCl3 evaporated to yield alpha-hydroxylauric acid.

후처리

  1. additionThe reaction mixture was poured into a separatory funnel, to which
  2. extractionThe mixture was extracted with chloroform
  3. customThe chloroform layer was removed
  4. customthe CHCl3 evaporated

출처 및 근거

ORD 기록
ord-39e27f2d4b784cdc8dd8f06831abdd2a
출처 데이터셋
uspto-grants-1984_09
특허 번호
US04469635

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