Benzyl Chloride → 1-Benzyl-3,4-diethylpyridin-1-ium chloride
반응식
[CH2:1]([Cl:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:9]([C:11]1[CH:12]=[N:13][CH:14]=[CH:15][C:16]=1[CH2:17][CH3:18])[CH3:10]>C(O)(C)C>[Cl-:8].[CH2:1]([N+:13]1[CH:14]=[CH:15][C:16]([CH2:17][CH3:18])=[C:11]([CH2:9][CH3:10])[CH:12]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1참가 물질
4
실험 절차
Benzyl chloride (250 g.) was added dropwise to a stirred and refluxed solution of 3,4-diethylpyridine (262 g.) and isopropyl alcohol (700 ml.). Repeated concentration under vacuum and addition of benzene afforded a slurry of crystalline 1-benzyl-3,4-diethyl-pyridinium chloride.
후처리
- concentrationconcentration
- additionunder vacuum and addition of benzene
출처 및 근거
- ORD 기록
- ord-84e712d38cec4785bd027dd88436149f
- 출처 데이터셋
- uspto-grants-1978_08
- 특허 번호
- US04108857
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