Phosphoric Acid → 3-Azidomethyl-2-thienylacetic Acid
반응식
[N:1]([CH2:4][C:5]1[CH:9]=[CH:8][S:7][C:6]=1[CH2:10][C:11]([O:13]CC)=[O:12])=[N+:2]=[N-:3].S(=O)(=O)(O)O.P(=O)(O)(O)O>>[N:1]([CH2:4][C:5]1[CH:9]=[CH:8][S:7][C:6]=1[CH2:10][C:11]([OH:13])=[O:12])=[N+:2]=[N-:3]참가 물질
4
실험 절차
Hydrolysis of ethyl 3-azidomethyl-2-thienylacetate by the above procedure or by employing an equal volume of 6M sulfuric acid or 8M phosphoric acid in place of the 3M hydrochloric acid also affords the title compound.
출처 및 근거
- ORD 기록
- ord-e142cf79ebb14fdebbfdaefbcbf217a0
- 출처 데이터셋
- uspto-grants-1978_08
- 특허 번호
- US04110342
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