Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 2-(3-methoxy-4-(5-nitroquinolin-6-yloxy)phenyl)acetate → Ethyl 2-(4-(5-aminoquinolin-6-yloxy)-3-methoxyphenyl)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 2-(3-methoxy-4-(5-nitroquinolin-6-yloxy)phenyl)acetate | HCID 59864865 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Ethyl 2-(4-(5-aminoquinolin-6-yloxy)-3-methoxyphenyl)acetate | HCID 59864773 | — |
반응 단계
Pd/C (30 mg) was added to 24.3 (310 mg) in EtOH (10 mL). The mixture was stirred under hydrogen at room temperature for 6 h. The catalyst was removed by filtration through celite. The filtrate was concentrated under vacuum to give 24.4. MS ESI (pos.) m/z: 353.1 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07960567B2 |
| 출처 데이터셋 | uspto-grants-2011_06 |
| ORD ID | ord-c8724ae8dfef40108eebf9c767ea9de2 |
| 출처 메모 | uspto-grants-2011_06 |