HRID2423318

反应详情

EQUATION

反应方程式

HRID 2423318 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Pd/C (30 mg) was added to 24.3 (310 mg) in EtOH (10 mL). The mixture was stirred under hydrogen at room temperature for 6 h. The catalyst was removed by filtration through celite. The filtrate was concentrated under vacuum to give 24.4. MS ESI (pos.) m/z: 353.1 (M+H).

WORKUP

后处理

  1. customThe catalyst was removed by filtration through celite
  2. concentrationThe filtrate was concentrated under vacuum