3-Nitrobenzoic acid → 4'-Fluoro-3-nitrobenzanilide

HRID 2441

반응식

HRID 2441 반응식
[F:1][C:2]1[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][CH:3]=1.[N+:9]([C:12]1[CH:13]=[C:14]([CH:18]=[CH:19][CH:20]=1)[C:15](O)=[O:16])([O-:11])=[O:10]>>[N+:9]([C:12]1[CH:13]=[C:14]([CH:18]=[CH:19][CH:20]=1)[C:15]([NH:6][C:5]1[CH:7]=[CH:8][C:2]([F:1])=[CH:3][CH:4]=1)=[O:16])([O-:11])=[O:10]

참가 물질

3

반응물 2

HCID 84973-Nitrobenzoic acidHCID 97314-Fluoroaniline

생성물 1

HCID 7652934'-Fluoro-3-nitrobenzanilide수율 76.1%

실험 절차

Using 4-fluoroaniline (1.1 ml, 10.9 mmol) and 3-nitrobenzoic acid (1.76 g, 10.0 mmol), the procedure of Reference Example 16 was repeated to obtain 1.98 g (76.0%) of the title compound in the form of light yellow needle crystals.

출처 및 근거

ORD 기록
ord-29a2732da3a948f4aae1ec2e95eeccf2
출처 데이터셋
uspto-grants-1998_03
특허 번호
US05728835

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