참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetone Cyanohydrin | HCID 6406 | — |
| 반응물 | p-Toluidine | HCID 7813 | — |
| 생성물 | 2-Methyl-2-[(4-methylphenyl)amino]propanenitrile | HCID 21239243 | 99% |
반응 단계
A mixture of p-toluidine (1.07 g, 10 mmol) and acetone cyanohydrin (10 ml) was heated to 80° C. and stirred for 4 h. The medium was concentrated and dried under vacuum to yield 2-methyl-2-(4-methylphenyl)aminopropanenitrile, 5a (1.72 g, 9.9 mmol, 99%) as brown solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08658681B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_02 |
|---|
| ORD ID | ord-2c9e85e79b0847ab9dc519139d06e06d |
|---|
| 출처 메모 | uspto-grants-2014_02 |
|---|
