Hydrochloric Acid → Methyl 2,6-dichlorophenylacetate

HRID 24671노트

반응식

HRID 24671 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1[CH2:9][C:10]([OH:12])=[O:11].Cl.[CH3:14]O>>[CH3:14][O:11][C:10](=[O:12])[CH2:9][C:3]1[C:2]([Cl:1])=[CH:7][CH:6]=[CH:5][C:4]=1[Cl:8]

참가 물질

4

반응물 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 810582,6-Dichlorophenylacetic acid

생성물 1

HCID 2734107Methyl 2,6-dichlorophenylacetate

실험 절차

(2,6-Dichlorophenyl)acetic acid (2.55 g) was dissolved in anhydrous MeOH (60 mL) and HCl (gas) was passed through the mixture and the resulting solution was stirred at room temperature for 18 h. The solvent was then evaporated to give (2,6-dichlorophenyl)acetic acid methyl ester (2.7 g).

후처리

  1. customThe solvent was then evaporated

출처 및 근거

ORD 기록
ord-90bb675ddfda4fec9b754c7947ac0371
출처 데이터셋
uspto-grants-2005_02
특허 번호
US06855843B2

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