Chlorine → Benzene, 2-chloro-1-fluoro-4-(trifluoromethyl)-

HRID 246899

반응식

HRID 246899 반응식
[F:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]([F:11])([F:10])[F:9])=[CH:4][C:3]=1[N+]([O-])=O.[Cl:15]Cl>>[Cl:15][C:3]1[CH:4]=[C:5]([C:8]([F:11])([F:10])[F:9])[CH:6]=[CH:7][C:2]=1[F:1]

참가 물질

3

반응물 2

HCID 24526ChlorineHCID 677784-Fluoro-3-nitrobenzotrifluoride

생성물 1

HCID 157153Benzene, 2-chloro-1-fluoro-4-(trifluoromethyl)-

반응 조건

온도
320 °C

실험 절차

In a continuous process, about 8 parts per hour of 4-fluoro-3-nitrobenzotrifluoride vapors and about 15 parts per hour of chlorine gas were passed simultaneously through a vapor phase reactor maintained at a temperature of about 320° C. and the reaction product vapors were condensed and collected. The process was continued until about 40 parts of 4-fluoro-3-nitrobenzotrifluoride had been passed through the reactor, yielding about 36.3 parts of 3-chloro-4-fluorobenzotrifluoride product. The structure of the product was confirmed by spectral analysis.

후처리

  1. customcondensed
  2. customcollected

출처 및 근거

ORD 기록
ord-6e8d9d79d995455cab8dcd5b56d5a2fd
출처 데이터셋
uspto-grants-1987_11
특허 번호
US04704483

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