Hydrochloric Acid → HCID 11780934, 화합물

HRID 247845노트

반응식

HRID 247845 반응식
[CH3:1][N:2]([CH:6]1[CH2:11][CH2:10][N:9]([CH2:12][CH2:13][CH2:14][CH2:15][O:16][C:17]2[CH:22]=[CH:21][C:20]([F:23])=[CH:19][CH:18]=2)[CH2:8][CH2:7]1)C(=O)C.Cl>CO>[F:23][C:20]1[CH:19]=[CH:18][C:17]([O:16][CH2:15][CH2:14][CH2:13][CH2:12][N:9]2[CH2:8][CH2:7][CH:6]([NH:2][CH3:1])[CH2:11][CH2:10]2)=[CH:22][CH:21]=1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 19764643N-Methyl-N-{1-[4-(p-fluorophenoxy)butyl]-4-piperidyl}acetamide

생성물 1

HCID 11780934HCID 11780934, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

0.05 mole of the compound obtained in stage D is refluxed for 12 hours in the presence of 570 cm3 of methanol and 340 cm3 of 5N hydrochloric acid. The methanol is evaporated and the mixture is poured into ice and then basified with sodium hydroxide. It is extracted with ether.

후처리

  1. customThe methanol is evaporated
  2. additionthe mixture is poured into ice
  3. extractionIt is extracted with ether

출처 및 근거

ORD 기록
ord-c01548b052cb476bb7336025740cb417
출처 데이터셋
uspto-grants-1993_05
특허 번호
US05208243

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