참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Iodoethane | HCID 6340 | — |
| 반응물 | N-(2-Pyridinylmethyl)-4-(tetradecyloxy)benzamide | HCID 10093859 | — |
| 생성물 | 1-Ethyl-2-[[[4-(tetradecyloxy)benzoyl]amino]methyl]pyridinium iodide | HCID 19016226 | — |
반응 단계
A mixture of 1.0 g of product from Example 4 and 9.42 ml of ethyl iodide is heated, in a sealed dark tube, at 140° C. for 20 hours. The cooled reaction mixture is concentrated in vacuo, the residue purified by column chromatography (silica gel:10% methyl alcohol/chloroform) and recrystallized from 5% chloroform/methyl alcohol to give 0.96 g of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05208247 |
|---|
| 출처 데이터셋 | uspto-grants-1993_05 |
|---|
| ORD ID | ord-58e62dd22d0241b4a70948708cab22d3 |
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| 출처 메모 | uspto-grants-1993_05 |
|---|
