Sodium Hydroxide → HCID 178452788, 화합물

HRID 24809

반응식

HRID 24809 반응식
C([N:4]1[C:12]2[C:7](=[CH:8][C:9]([N+:13]([O-:15])=[O:14])=[CH:10][CH:11]=2)[C:6](=[C:16](OC)[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[C:5]1=[O:25])(=O)C.[C:26]([O:30][C:31]([NH:33][C:34]1[CH:40]=[CH:39][C:37]([NH2:38])=[CH:36][CH:35]=1)=[O:32])([CH3:29])([CH3:28])[CH3:27].[OH-].[Na+]>CN(C=O)C.CO>[C:26]([O:30][C:31]([NH:33][C:34]1[CH:35]=[CH:36][C:37]([NH:38]/[C:16](=[C:6]2\[C:5](=[O:25])[NH:4][C:12]3[C:7]\2=[CH:8][C:9]([N+:13]([O-:15])=[O:14])=[CH:10][CH:11]=3)/[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[CH:39][CH:40]=1)=[O:32])([CH3:29])([CH3:27])[CH3:28]

참가 물질

6

반응물 3

HCID 14798Sodium HydroxideHCID 688611tert-Butyl (4-aminophenyl)carbamateHCID 541401551-Acetyl-3-(1-methoxy-1-phenyl-methylidene)-5-nitro-2-indolinone

생성물 1

HCID 178452788HCID 178452788, 화합물

시약·촉매·용매 2

HCID 887Methanol용매HCID 6228Dimethylformamide용매

실험 절차

Prepared analogously to Example 82 from 1-acetyl-3-(1-methoxy-1-phenyl-methylidene)-5-nitro-2-indolinone and 4-tert.butoxycarbonylamino-aniline in DMF and subsequent treatment with sodium hydroxide solution in methanol.

출처 및 근거

ORD 기록
ord-c00a7cb5bdf94b7983b3c440073516b0
출처 데이터셋
uspto-grants-2005_02
특허 번호
US06855710B2

연결된 노트

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