Hydrochloric Acid → HCID 22569398, 화합물

HRID 24942노트

반응식

HRID 24942 반응식
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[CH3:11][N:12]([CH3:16])[CH2:13][CH2:14][NH2:15].Cl>C(O)C>[CH3:11][N:12]([CH3:16])[CH2:13][CH2:14][NH:15][C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 9590p-FluoronitrobenzeneHCID 66053N,N-Dimethylethylenediamine

생성물 1

HCID 22569398HCID 22569398, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

2.2 ml of (20 mmol) of 4-fluoronitrobenzene and 2.6 ml (24 mmol) of N,N-dimethylethylene-diamine are heated in 10 ml of ethanol at 120° C. in a microwave oven for 1.5 hours. Then 50 ml of 1 N hydrochloric acid are added. The reaction solution is washed with ethyl acetate. Then the aqueous phase is combined with 4 N sodium hydroxide solution until an alkaline reaction is obtained and extracted with ethyl acetate.

후처리

  1. washThe reaction solution is washed with ethyl acetate
  2. customThen the aqueous phase is combined with 4 N sodium hydroxide solution until an alkaline reaction
  3. customis obtained
  4. extractionextracted with ethyl acetate

출처 및 근거

ORD 기록
ord-33970417aed54766919fad76ccaaf316
출처 데이터셋
uspto-grants-2005_02
특허 번호
US06855710B2

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