참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methyl isothiocyanate | HCID 11167 | — |
| 반응물 | Ethyl[(pyridin-3-yl)methyl]amine | HCID 4716480 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | N-methyl-N'-ethyl-N'-(3-pyridylmethyl)thiourea | HCID 22450434 | 100.3% |
반응 단계
In 50 ml of ethyl ether was dissolved 2.4 g of N-ethyl-N-(3-pyridylmethyl)amine followed by addition of 1.3 g of methyl isothiocyanate. The mixture was stirred at room temperature (25° C.) for 1 hour. The resulting precipitate was collected by filtration, washed with a small amount of ethyl ether and dried to give 3.7 g of N-methyl-N'-ethyl-N'-(3-pyridylmethyl)thiourea as white prisms.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05214152 |
|---|
| 출처 데이터셋 | uspto-grants-1993_05 |
|---|
| ORD ID | ord-44541d504266468eb6785c420de3fa6e |
|---|
| 출처 메모 | uspto-grants-1993_05 |
|---|
