Glycine ethyl ester → Ethyl 2-(2-hydroxy-3-methoxypropylamino)acetate

HRID 25038

반응식

HRID 25038 반응식
[CH3:1][O:2][CH2:3][CH:4]1[O:6][CH2:5]1.[CH2:7]([O:9][C:10](=[O:13])[CH2:11][NH2:12])[CH3:8]>C(O)C>[OH:6][CH:4]([CH2:3][O:2][CH3:1])[CH2:5][NH:12][CH2:11][C:10]([O:9][CH2:7][CH3:8])=[O:13]

참가 물질

4

반응물 2

HCID 12176Glycine ethyl esterHCID 135891,2-Epoxy-3-methoxypropane

생성물 1

HCID 21922545Ethyl 2-(2-hydroxy-3-methoxypropylamino)acetate수율 100%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A solution of glycidyl methyl ether (1.00 g) and glycine ethyl ester (5.91 g) in ethanol was stirred overnight, and concentrated under reduced pressure to obtain the title compound (2.17 g).

후처리

  1. concentrationconcentrated under reduced pressure

출처 및 근거

ORD 기록
ord-375d93cfbe1742b5bc1217472b0ae0b6
출처 데이터셋
uspto-grants-2005_02
특허 번호
US06858599B2

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