Glycine → HCID 66712759, 화합물

HRID 250402노트

반응식

HRID 250402 반응식
[F:1][C:2]([F:16])([F:15])[C:3]1[CH:4]=[C:5]([C:12]([OH:14])=O)[C:6](=[CH:10][CH:11]=1)[C:7]([OH:9])=O.[NH2:17][CH2:18][C:19]([OH:21])=[O:20].[CH3:22]O>>[CH3:22][O:20][C:19](=[O:21])[CH2:18][N:17]1[C:12](=[O:14])[C:5]2[C:6](=[CH:10][CH:11]=[C:3]([C:2]([F:1])([F:16])[F:15])[CH:4]=2)[C:7]1=[O:9]

참가 물질

4

반응물 3

HCID 750GlycineHCID 887MethanolHCID 5990394-(Trifluoromethyl)phthalic acid

생성물 1

HCID 66712759HCID 66712759, 화합물

실험 절차

4-trifluoromethyl-phthalic acid was reacted with glycine in analogy to Example D-1 b). The crude product was then reacted with methanol in analogy to Example D-1 c); 1H NMR (CDCl3): δ=8.14 (s, 1H), 8.02 (m, 2H), 4.48 (s, 2H), 3.78 (s, 3H).

출처 및 근거

ORD 기록
ord-ba4902732ce441f68b37c78c88bd83d5
출처 데이터셋
uspto-grants-2011_01
특허 번호
US07863292B2

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