Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Azobisisobutyronitrile → Styrenesulfonic Acid Allylhexafluoro-Isopropanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Azobisisobutyronitrile | HCID 6547 | — |
| 반응물 | 4-Penten-2-ol, 1,1,1-trifluoro-2-(trifluoromethyl)- | HCID 328870 | — |
| 반응물 | Sodium styrenesulfonate | HCID 53627496 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | Styrenesulfonic Acid Allylhexafluoro-Isopropanol | HCID 131728620 | — |
반응 단계
19 g of sodium styrenesulfonate (SSNa) (available from Sigma-Aldrich Corp.) and 1 g of 2-Allylhexafluoro-isopropanol are fully dissolved in 0.24 L of dimethylsulfoxide (DMSO) with heating. Then, 0.1 g of azobisisobutyronitrile (AIBN) is added dropwise to the DMSO solution. The monomers are polymerized for 24 hours or more. The polymerization is carried out varying the content of the allylhexafluoro-isopropanol (2, 5, 10, and 20 wt %).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07875208B2 |
| 출처 데이터셋 | uspto-grants-2011_01 |
| ORD ID | ord-ed02a1056370470d86ee721b3d2d6bbb |
| 출처 메모 | uspto-grants-2011_01 |