Ethylenediamine → 2-(2,6-Dicyclopropyl-benzyl)-4,5-dihydro-1H-imidazole

HRID 254537노트

반응식

HRID 254537 반응식
[CH:1]1([C:4]2[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]3[CH2:12][CH2:11]3)[C:5]=2[CH:13]=[C:14](Br)Br)[CH2:3][CH2:2]1.[CH2:17]([NH2:20])[CH2:18][NH2:19]>>[CH:1]1([C:4]2[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]3[CH2:12][CH2:11]3)[C:5]=2[CH2:13][C:14]2[NH:19][CH2:18][CH2:17][N:20]=2)[CH2:3][CH2:2]1

참가 물질

3

반응물 2

HCID 3301EthylenediamineHCID 589517651,3-Dicyclopropyl-2-(2,2-dibromo-vinyl)-benzene

생성물 1

HCID 589517102-(2,6-Dicyclopropyl-benzyl)-4,5-dihydro-1H-imidazole

실험 절차

2-(2,6-Dicyclopropyl-benzyl)-4,5-dihydro-1H-imidazole was prepared from 1,3-dicyclopropyl-2-(2,2-dibromo-vinyl)-benzene and ethylenediamine in analogy to Example 1e): light yellow crystals; MS (ISP): 241.4 ([M+H]+, 100%).

출처 및 근거

ORD 기록
ord-eaf78f8da7bd4aea8ac60bb95d585863
출처 데이터셋
uspto-grants-2011_01
특허 번호
US07875645B2

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