Cyanamide → HCID 86619051, 화합물

HRID 255127노트

반응식

HRID 255127 반응식
[F:1][C:2]([F:8])([F:7])[CH2:3][CH2:4][CH:5]=O.N1CCCC1.O.C1(C)C=CC([S:21](O)(=O)=O)=CC=1.[S].[N:27]#[C:28][NH2:29]>>[F:1][C:2]([F:8])([F:7])[CH2:3][C:4]1[S:21][C:28]([NH2:29])=[N:27][CH:5]=1

참가 물질

6

반응물 5

HCID 9864CyanamideHCID 31268PyrrolidineHCID 521998p-Toluenesulfonic acid monohydrateHCID 27770834,4,4-TrifluorobutanalHCID 5362487Sulfur

생성물 1

HCID 86619051HCID 86619051, 화합물

실험 절차

A mixture of 4,4,4-trifluorobutyraldehyde (Matrix), pyrrolidine, p-toluenesulfonic acid monohydrate, sulfur and cyanamide were processed using the method described in Example 136A to obtain the title compound. MS (ESI+) m/z 183 (M+H)+.

출처 및 근거

ORD 기록
ord-d761a2f406114e86992dfc1ff0d839d1
출처 데이터셋
uspto-grants-2011_01
특허 번호
US07875639B2

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