1-(2-Nitro-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane → HCID 20165755, 화합물

HRID 255461

반응식

HRID 255461 반응식
[N+:1]([C:4]([CH3:17])([CH3:16])[CH2:5][O:6][CH:7]1[C:11]([CH3:13])([CH3:12])[CH2:10][CH2:9][C:8]1([CH3:15])[CH3:14])([O-])=O>CO.[Ni]>[NH2:1][C:4]([CH3:17])([CH3:16])[CH2:5][O:6][CH:7]1[C:11]([CH3:13])([CH3:12])[CH2:10][CH2:9][C:8]1([CH3:15])[CH3:14]

참가 물질

4

반응물 1

HCID 201657161-(2-Nitro-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane

생성물 1

HCID 20165755HCID 20165755, 화합물

시약·촉매·용매 2

HCID 935Nickel촉매HCID 887Methanol용매

실험 절차

1-(2-Nitro-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane is dissolved in methanol and hydrogenated at 50 psi with Raney nickel T-1 as a catalyst. The reaction mixture is filtered through Celite and evaporated to yield 1-(2-amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane.

후처리

  1. filtrationThe reaction mixture is filtered through Celite
  2. customevaporated

출처 및 근거

ORD 기록
ord-072cd696dd184a92a527b40d5e77fb5d
출처 데이터셋
uspto-grants-1987_10
특허 번호
US04698231

연결된 노트

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