Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trifluoroacetic acid → HCID 178484796, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trifluoroacetic acid | HCID 6422 | — |
| 반응물 | HCID 178486032 | HCID 178486032 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 178484796 | HCID 178484796 | 166.6% |
반응 단계
200 mg (0.53 mmol) of trans-Methansulfonic acid 5[-4-(tert-butoxy carbonyl-methyl-amino)-cyclohexyl)-pentyl ester, dissolved in 2 ml of CH2Cl2, was treated with 2 ml of TFA. After stirring for 20 min at RT, the solution was concentrated in vacuo to yield 245 mg of pure trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentylester.trifluoroacetic acid salt, MS: 278 (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06858651B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-5ac50a9b73ce4cf084179954503a48e5 |
| 출처 메모 | uspto-grants-2005_02 |