참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phosphorus tribromide | HCID 24614 | — |
| 반응물 | (2,2,5,5-Tetramethylcyclopentyl)methanol | HCID 13629260 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 2,2,5,5-Tetramethyl-1-cyclopentylmethylbromide | HCID 13629261 | — |
반응 단계
2,2,5,5-Tetramethyl-1-cyclopentylmethanol is dissolved in benzene and stirred at 0° C. under argon. A solution of phosphorus tribromide in benzene is added and the mixture is stirred for 2 hours and then heated to 60° C. for 4 hours. The mixture is cooled, poured into ice and extracted with ether. The organic layer is washed with saturated NaHCO3, dried over MgSO4 and evaporated to yield 2,2,5,5-Tetramethyl-1-cyclopentylmethyl bromide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04701552 |
|---|
| 출처 데이터셋 | uspto-grants-1987_10 |
|---|
| ORD ID | ord-b24f7ef350984c38b2b104737856de51 |
|---|
| 출처 메모 | uspto-grants-1987_10 |
|---|
