Acetic Anhydride → HCID 19785474, 화합물
반응식
[ClH:1].Cl.[N:3]12[CH2:10][CH2:9][CH:6]([CH2:7][CH2:8]1)[CH:5]([O:11][C:12]1[CH:17]=[CH:16][C:15]([NH2:18])=[CH:14][CH:13]=1)[CH2:4]2.[C:19](OC(=O)C)(=[O:21])[CH3:20]>N1C=CC=CC=1>[ClH:1].[N:3]12[CH2:8][CH2:7][CH:6]([CH2:9][CH2:10]1)[CH:5]([O:11][C:12]1[CH:17]=[CH:16][C:15]([NH:18][C:19](=[O:21])[CH3:20])=[CH:14][CH:13]=1)[CH2:4]2참가 물질
4
실험 절차
4-[(1-azabicyclo[2.2.2]oct-3-yl)oxy]benzenamine (Example 3) was acetylated with acetic anhydride in dry pyridine at -10° C. The crude product was converted into the hydrochloric salt to obtain N-[4-[(1-azabicyclo[2.2.2]-oct-3-yl)oxy]phenyl]acetamide hydrochloride. M.p. >250° C.
출처 및 근거
- ORD 기록
- ord-a68130013335449db4b8ecfabc11a40b
- 출처 데이터셋
- uspto-grants-1993_11
- 특허 번호
- US05258392
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