Methyl iodide → 131988-12-0

HRID 256925노트

반응식

HRID 256925 반응식
[CH3:1][I:2].[CH2:3]([O:5][C:6]1[C:7]([C:11]2[CH:12]=[N:13][CH:14]=[CH:15][CH:16]=2)=[N:8][S:9][N:10]=1)[CH3:4]>CC(C)=O>[I-:2].[CH2:3]([O:5][C:6]1[C:7]([C:11]2[CH:12]=[N+:13]([CH3:1])[CH:14]=[CH:15][CH:16]=2)=[N:8][S:9][N:10]=1)[CH3:4]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 15180131Pyridine, 3-(4-ethoxy-1,2,5-thiadiazol-3-yl)- (9CI)

생성물 1

HCID 15819042131988-12-0

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(4-ethoxy-1,2,5-thiadiazol-3-yl)pyridine (520 mg, 2.5 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.72 g (83%).

후처리

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.72 g (83%)

출처 및 근거

ORD 기록
ord-c6ef184dca474ec6ac95906eed20063b
출처 데이터셋
uspto-grants-1993_11
특허 번호
US05260311

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