Methyl iodide → HCID 70144934, 화합물

HRID 256970노트

반응식

HRID 256970 반응식
[CH3:1][I:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)/[CH:4]=[CH:5]\[CH2:6][CH3:7]>CC(C)=O>[I-:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)/[CH:4]=[CH:5]\[CH2:6][CH3:7]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 70145705HCID 70145705, 화합물

생성물 1

HCID 70144934HCID 70144934, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A mixture of methyl iodide (1 ml, 15 mmol) and cis-3-(4-(2-pentenyloxy)-1,2,5-thiadiazol-3-yl) pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.53 g (46%).

후처리

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.53 g (46%)

출처 및 근거

ORD 기록
ord-25da0a07372042b9852d52c28f76bbde
출처 데이터셋
uspto-grants-1993_11
특허 번호
US05260311

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