Methyl iodide → HCID 70144872, 화합물

HRID 256972노트

반응식

HRID 256972 반응식
[CH3:1][I:2].[CH2:3]([O:9][C:10]1[C:11]([C:15]2[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)/[CH:4]=[CH:5]\[CH2:6][CH2:7][CH3:8]>CC(C)=O>[I-:2].[CH2:3]([O:9][C:10]1[C:11]([C:15]2[CH:16]=[N+:17]([CH3:1])[CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)/[CH:4]=[CH:5]\[CH2:6][CH2:7][CH3:8]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 70144708HCID 70144708, 화합물

생성물 1

HCID 70144872HCID 70144872, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A mixture of methyl iodide (0.5 ml, 7.5 mmol) and cis-3-(4-(2-hexenyloxy)-1, 2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (4 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration.

후처리

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration

출처 및 근거

ORD 기록
ord-37adedb778284d1b85a0fc809bd8379d
출처 데이터셋
uspto-grants-1993_11
특허 번호
US05260311

반응 노트

불러오는 중…