4-Ethylpyridine → 1-(2,6-Dichlorophenyl)-3-(4-pyridyl)butane

HRID 257467

반응식

HRID 257467 반응식
[CH2:1]([C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1)[CH3:2].[Cl:9][C:10]1[CH:18]=[CH:17][CH:16]=[C:15]([Cl:19])[C:11]=1[CH2:12][CH2:13]Br>>[Cl:9][C:10]1[CH:18]=[CH:17][CH:16]=[C:15]([Cl:19])[C:11]=1[CH2:12][CH2:13][CH:1]([C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1)[CH3:2]

참가 물질

3

반응물 2

HCID 108224-EthylpyridineHCID 134801952-(2-Bromoethyl)-1,3-dichlorobenzene

생성물 1

HCID 197833131-(2,6-Dichlorophenyl)-3-(4-pyridyl)butane수율 55.3%

실험 절차

1.0 g (9.35 mmol) of 4-ethylpyridine and 2.37 g (9.35 mmol) of 2,6-dichlorophenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.45 g of the desired compound (yield: 55.3%). The resulting compound was identified as 1-(2,6-dichlorophenyl)-3-(4-pyridyl)-butane (hereinafter referred to as compound 11) by the following analytical results.

후처리

  1. customThe reaction product was purified

출처 및 근거

ORD 기록
ord-ee4c7f6b2d9949818626607b3a34d2d8
출처 데이터셋
uspto-grants-1993_11
특허 번호
US05262420

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