Methyl iodide → HCID 70144872, 화합물

HRID 257910노트

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HRID 257910 반응식
[CH3:1][I:2].[CH2:3]([O:9][C:10]1[C:11]([C:15]2[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)/[CH:4]=[CH:5]\[CH2:6][CH2:7][CH3:8]>CC(C)=O>[I-:2].[CH2:3]([O:9][C:10]1[C:11]([C:15]2[CH:16]=[N+:17]([CH3:1])[CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)/[CH:4]=[CH:5]\[CH2:6][CH2:7][CH3:8]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 70144708HCID 70144708, 화합물

생성물 1

HCID 70144872HCID 70144872, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A mixture of methyl iodide (0.5 ml, 7.5 mmol) and cis-3-(4-(2-hexenyloxy)-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (4 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration.

후처리

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration

출처 및 근거

ORD 기록
ord-883799c149a34a6a871c92e841eea320
출처 데이터셋
uspto-grants-1993_11
특허 번호
US05264444

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