Methyl iodide → HCID 19075326, 화합물

HRID 257929

반응식

HRID 257929 반응식
[CH3:1][I:2].[CH2:3]([O:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][O:11][C:12]1[C:13]([C:17]2[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=2)=[N:14][S:15][N:16]=1)[CH3:4]>CC(C)=O>[I-:2].[CH2:3]([O:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][O:11][C:12]1[C:13]([C:17]2[CH:18]=[N+:19]([CH3:1])[CH:20]=[CH:21][CH:22]=2)=[N:14][S:15][N:16]=1)[CH3:4]

참가 물질

4

실험 절차

A mixture of methyl iodide (0.5 ml, 9 mmol) and 3-(4-(2-(2-ethoxyethoxy)ethoxy)-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration.

후처리

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration

출처 및 근거

ORD 기록
ord-47ac09cde6f54f13bd021f87271ed437
출처 데이터셋
uspto-grants-1993_11
특허 번호
US05264444

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