Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isoquinoline → HCID 21425396, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isoquinoline | HCID 8405 | — |
| 반응물 | 2-Bromo-1,2-diphenylethan-1-one | HCID 102630 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | HCID 21425396 | HCID 21425396 | — |
반응 단계
A solution of isoquinoline(10 g) and desylbromide (10 g) in dry benzene (50 ml) was stirred at 40° for seven hours. The suspension was allowed to stand overnight, and the benzene solution decanted off. The solid was ground to a powder, washed well with ether, and dried. Yield 12.3 g (85%), m.p. 239°-241° (Found C 68.3; H 4.6; N 3.4, Required C 68.3; H 4.5; N 3.5).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04035499 |
| 출처 데이터셋 | uspto-grants-1977_07 |
| ORD ID | ord-c0caa46ece104cd28f97510ceffa0466 |
| 출처 메모 | uspto-grants-1977_07 |