Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetaldehyde → Phenyl[1-(piperidinosulfonylamino)ethyl]phenylphosphinate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetaldehyde | HCID 177 | — |
| 반응물 | Diphenyl phenylphosphonite | HCID 239038 | — |
| 반응물 | 1-Piperidinesulfonamide | HCID 276741 | — |
| 용매 | Chlorobenzene | HCID 7964 | — |
| 생성물 | Phenyl[1-(piperidinosulfonylamino)ethyl]phenylphosphinate | HCID 21428537 | 75% |
반응 단계
This compound is obtained in 75% yield in a crude form from a mixture of equimolar quantities of diphenyl phenylphosphonite, acetaldehyde, and piperidinosulfonylamine in chlorobenzene. Recrystallization of a portion twice from acetonitrile gives a white solid product: mp 152°-165°; 31P nmr(DMSO-d6) -38.4 ppm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04036913 |
| 출처 데이터셋 | uspto-grants-1977_07 |
| ORD ID | ord-10282a474b3343a584316eff86c987e8 |
| 출처 메모 | uspto-grants-1977_07 |