Phenyl Isothiocyanate → HCID 12939879, 화합물

반응식

[Br:1][C:2]1[CH:12]=[CH:11][C:5]([CH2:6][NH:7][CH:8]([CH3:10])[CH3:9])=[CH:4][CH:3]=1.[C:13]1([N:19]=[C:20]=[S:21])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:6][N:7]([CH:8]([CH3:9])[CH3:10])[C:20]([NH:19][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[S:21])=[CH:11][CH:12]=1

참가 물질

반응물 2

HCID 7673Phenyl Isothiocyanate

HCID 12939866(4-Bromobenzyl)isopropylamine

생성물 1

HCID 12939879HCID 12939879, 화합물수율 88%

실험 절차

Following the procedure described in Example 1, process variant (a), 23 g of N-(4-bromobenzyl)-N-isopropylamine were reacted with 14 g of phenyl isothiocyanate. 32 g of N-(4-bromobenzyl)-N-isopropyl-N'-phenylthiourea were obtained. Yield: 88%. Melting point: 133.5°-134.5° C.

출처 및 근거

ORD 기록: ord-05a6e7f3fd2d40379bbe6e598ce0085c
출처 데이터셋: uspto-grants-1977_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04036986

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