2-Ethylhexylamine → 2-cyano-N-(2-ethylhexyl)acetamide

HRID 259376

반응식

HRID 259376 반응식
C(O[C:4](=[O:8])[CH2:5][C:6]#[N:7])C.[CH2:9]([CH:11]([CH2:14][CH2:15][CH2:16][CH3:17])[CH2:12][NH2:13])[CH3:10]>C(O)C>[CH2:9]([CH:11]([CH2:14][CH2:15][CH2:16][CH3:17])[CH2:12][NH:13][C:4](=[O:8])[CH2:5][C:6]#[N:7])[CH3:10]

참가 물질

4

반응물 2

HCID 77192-EthylhexylamineHCID 7764Ethyl cyanoacetate

생성물 1

HCID 45907042-cyano-N-(2-ethylhexyl)acetamide

시약·촉매·용매 1

HCID 702Ethanol용매

반응 조건

온도
154 °C

실험 절차

To ethylcyanoacetate (141 g., 1.25 mole) is slowly added 2-ethylhexylamine (129 g., 1.0 mole) over a period of 0.5 hours. The solution is then gradually heated to 154° C. and the ethanol formed is collected over a period of 1.75 hours. The solution is then stripped of all volatiles boiling at or below 88° C./3.0 mm to give N-(2-ethylhexyl)cyanoacetamide, 201.5 g.

후처리

  1. customof 0.5 hours
  2. customis collected over a period of 1.75 hours
  3. custombelow 88° C./3.0 mm

출처 및 근거

ORD 기록
ord-f98c1453371a44e88d48735337fef260
출처 데이터셋
uspto-grants-1977_07
특허 번호
US04038065

연결된 노트

불러오는 중…