Dimethyldithiocarbamic acid, dimethylamine → p-Isopropyl-alpha-(nitromethyl)benzyl dimethyldithiocarbamate
반응식
[CH:1]([C:4]1[CH:14]=[CH:13][C:7]([CH:8]=[CH:9][N+:10]([O-:12])=[O:11])=[CH:6][CH:5]=1)([CH3:3])[CH3:2].[CH3:15][N:16]([CH3:20])[C:17](=[S:19])[S-:18].C[NH2+]C>C(=S)=S>[CH3:15][N:16]([CH3:20])[C:17](=[S:18])[S:19][CH:8]([CH2:9][N+:10]([O-:12])=[O:11])[C:7]1[CH:13]=[CH:14][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:5][CH:6]=1참가 물질
4
실험 절차
As in Example 17, reaction of p-isopropyl-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave p-isopropyl-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 119° - 120° C. after recrystallization without heating from acetone-methanol solution.
출처 및 근거
- ORD 기록
- ord-9f9715b881c94eaca65b08adc465a367
- 출처 데이터셋
- uspto-grants-1977_07
- 특허 번호
- US04038288
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