Benzene → Isobutylidenebenzhydrylamine
반응식
[CH:1](=O)[CH:2]([CH3:4])[CH3:3].[CH:6]([NH2:19])([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1.C1C=CC=CC=1>O>[CH:1](=[N:19][CH:6]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH:2]([CH3:4])[CH3:3]참가 물질
5
실험 절차
14.4 parts of isobutyraldehyde was added to 36.6 parts of benzhydrylamine in 100 parts of dry benzene at room temperature with stirring. The cloudy mixture was heated to reflux with water-separation for 4 hours. On cooling the solution was filtered to remove a small amount of solid and evaporated to give isobutylidenebenzhydrylamine.
후처리
- temperatureThe cloudy mixture was heated
- temperatureOn cooling the solution
- filtrationwas filtered
- customto remove a small amount of solid
- customevaporated
출처 및 근거
- ORD 기록
- ord-c6b653a08d6e4a9db8afca08018af3b1
- 출처 데이터셋
- uspto-grants-1979_04
- 특허 번호
- US04147780
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