Benzene → Isobutylidenebenzhydrylamine

HRID 25972

반응식

HRID 25972 반응식
[CH:1](=O)[CH:2]([CH3:4])[CH3:3].[CH:6]([NH2:19])([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1.C1C=CC=CC=1>O>[CH:1](=[N:19][CH:6]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH:2]([CH3:4])[CH3:3]

참가 물질

5

반응물 3

HCID 241BenzeneHCID 6561IsobutyraldehydeHCID 7036Benzhydrylamine

생성물 1

HCID 10657527Isobutylidenebenzhydrylamine

시약·촉매·용매 1

HCID 962Water용매

실험 절차

14.4 parts of isobutyraldehyde was added to 36.6 parts of benzhydrylamine in 100 parts of dry benzene at room temperature with stirring. The cloudy mixture was heated to reflux with water-separation for 4 hours. On cooling the solution was filtered to remove a small amount of solid and evaporated to give isobutylidenebenzhydrylamine.

후처리

  1. temperatureThe cloudy mixture was heated
  2. temperatureOn cooling the solution
  3. filtrationwas filtered
  4. customto remove a small amount of solid
  5. customevaporated

출처 및 근거

ORD 기록
ord-c6b653a08d6e4a9db8afca08018af3b1
출처 데이터셋
uspto-grants-1979_04
특허 번호
US04147780

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