Phosphorus oxychloride → HCID 22401591, 화합물

반응식

[CH2:1]([C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]=1[NH2:13])[CH3:2].C([N:17]1[CH2:21][CH2:20][NH:19][C:18]1=O)(=O)C.O=P(Cl)(Cl)Cl>>[CH2:1]([C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]=1[NH:13][C:18]1[NH:19][CH2:20][CH2:21][N:17]=1)[CH3:2]

참가 물질

반응물 3

HCID 24813Phosphorus oxychloride

HCID 79350N-Acetylimidazolidinone

HCID 422871HCID 422871, 화합물

생성물 1

HCID 22401591HCID 22401591, 화합물

실험 절차

2-Ethylnaphthyl amine is reacted with N-acetyl-2imidazolidinone in the presence of POCl3 to produce the imidazoline intermediate. This intermediate is treated with sodium hydroxide and water to remove the aceto group and yield the name compound (VIII).

출처 및 근거

ORD 기록: ord-e02f8465e06a47d0b19e7413c530f73b
출처 데이터셋: uspto-grants-1996_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05527830

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