Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methoxyisonicotinonitrile → (2-Methoxypyridin-4-yl)methanamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methoxyisonicotinonitrile | HCID 7204887 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | (2-Methoxypyridin-4-yl)methanamine | HCID 16227983 | — |
반응 단계
A solution of 4-cyano-2-methoxypyridine (0.55 g, 4.1 mmol) in ethanol was hydrogenated at 60 psi H2 in the presence of 10% Pd/C (100 mg). After 3.5 h the catalyst was removed by filtration through Super-Gel and the liltrate evaporated to give the title compound as a foam.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05527819 |
| 출처 데이터셋 | uspto-grants-1996_06 |
| ORD ID | ord-3fa0020c6e9c4e56a9b2fcba963c000d |
| 출처 메모 | uspto-grants-1996_06 |