Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Beta-Nitrostyrene → alpha-(Nitromethyl)benzyl diethyldithiocarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Beta-Nitrostyrene | HCID 7626 | — |
| 반응물 | Diethylammonium diethylcarbamodithioate | HCID 2735004 | — |
| 용매 | Carbon Disulfide | HCID 6348 | — |
| 생성물 | alpha-(Nitromethyl)benzyl diethyldithiocarbamate | HCID 21324593 | — |
반응 단계
As in Example 17, reaction of β-nitrostyrene with diethylammonium diethyldithiocarbamate in the presence of carbon disulfide gave α-(nitromethyl)benzyl diethyldithiocarbamate melting at 81° C.-82.5° C. when recrystallized without heating from acetone-2-propanol solution.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04148795 |
| 출처 데이터셋 | uspto-grants-1979_04 |
| ORD ID | ord-021db1f139f940299dd9a715ed39cc5e |
| 출처 메모 | uspto-grants-1979_04 |