Azobisisobutyronitrile → Acrylamido methyl-4-hydroxy benzophenone stearyl methacrylate

HRID 261465

반응식

HRID 261465 반응식
[Pb].[N].[C:3]([NH:7][CH2:8][C:9]1[CH:22]=[C:21]([OH:23])[CH:20]=[CH:19][C:10]=1[C:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[O:12])(=[O:6])[CH:4]=[CH2:5].[C:24]([O:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH3:47])(=[O:28])[C:25]([CH3:27])=[CH2:26].N(C(C)(C)C#N)=NC(C)(C)C#N>CC(C)=O>[C:3]([NH:7][CH2:8][C:9]1[CH:22]=[C:21]([OH:23])[CH:20]=[CH:19][C:10]=1[C:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[O:12])(=[O:6])[CH:4]=[CH2:5].[C:24]([O:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH3:47])(=[O:28])[C:25]([CH3:27])=[CH2:26]

참가 물질

6

반응물 4

HCID 6547AzobisisobutyronitrileHCID 122600Stearyl methacrylateHCID 54571820Acrylamido methyl 4-hydroxy benzophenoneHCID 178514658HCID 178514658, 화합물

생성물 1

HCID 86733966Acrylamido methyl-4-hydroxy benzophenone stearyl methacrylate

시약·촉매·용매 1

HCID 180Acetone용매

반응 조건

온도
80 °C

실험 절차

Into a 50 ml flask provided with a condenser, a nitrogen lead in tube and an agitator, there are intorduced 1 g of acrylamido methyl 4-hydroxy benzophenone, 1.5 g of stearyl methacrylate and 0.25 g of azobis-isobutyronitrile in solution in 5 ml of acetone. The resulting mixture is heated for 8 hours at 80° C.

후처리

  1. customInto a 50 ml flask provided with a condenser

출처 및 근거

ORD 기록
ord-ad05431320e545f5b396ab21c0d42f84
출처 데이터셋
uspto-grants-1979_08
특허 번호
US04166109

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