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4-(4-Benzamidobutyl)-5-methylimidazole-2-thione → 4-(4-Benzamidobutyl)-5-methylimidazole

HRID 261623
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인쇄 미리보기

반응식

HRID 261623 반응식
[C:1]([NH:9][CH2:10][CH2:11][CH2:12][CH2:13][C:14]1[C:18]([CH3:19])=[N:17][C:16](=S)[N:15]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C(O)C.[Ni]>[C:1]([NH:9][CH2:10][CH2:11][CH2:12][CH2:13][C:14]1[N:15]=[CH:16][NH:17][C:18]=1[CH3:19])(=[O:8])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 1

HCID 203945574-(4-Benzamidobutyl)-5-methylimidazole-2-thione

생성물 1

HCID 127698434-(4-Benzamidobutyl)-5-methylimidazole수율 88.1%

시약·촉매·용매 2

HCID 935Nickel촉매HCID 702Ethanol용매

실험 절차

4-(4-Benzamidobutyl)-5-methylimidazole-2-thione (4.12 g, 0.01425 mol) in absolute ethanol (80 ml) was desulphrised with Raney nickel (approximately 18 g). Filtration followed by concentration under reduced pressure gave 4-(4-benzamidobutyl)-5-methylimidazole (3.23 g, 88%) m.p. 124°-128°.

후처리

  1. filtrationFiltration
  2. concentrationfollowed by concentration under reduced pressure

출처 및 근거

ORD 기록
ord-6628fa50f0e24f84a78fd204c0358e32
출처 데이터셋
uspto-grants-1979_08
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04166184

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