Stearoyl chloride → 2-Chlorostearoyl chloride

HRID 26169

반응식

HRID 26169 반응식
[C:1]([Cl:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].ClCl.[Cl:23]S(O)(=O)=O.C1C(=C(C#N)C#N)C=CC(=C(C#N)C#N)C=1>>[Cl:23][CH:2]([CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])[C:1]([Cl:20])=[O:19]

참가 물질

5

반응물 4

HCID 8212Stearoyl chlorideHCID 24526ChlorineHCID 24638Chlorosulfonic acidHCID 73697Tetracyanoquinodimethane

생성물 1

HCID 205126172-Chlorostearoyl chloride

실험 절차

Following the procedure of Example I, stearoyl chloride is reacted with chlorine in the presence of ClSO3H and TCNQ. The product is distilled to provide substantially pure 2-chlorostearoyl chloride.

후처리

  1. distillationThe product is distilled

출처 및 근거

ORD 기록
ord-4b0992e459a24daaa1b21148f6ab2d51
출처 데이터셋
uspto-grants-1979_04
특허 번호
US04148811

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