Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetonitrile → (4-Carboxybutyl)triphenylphosphonium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetonitrile | HCID 6342 | — |
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 반응물 | 5-Bromovaleric acid | HCID 16368 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | (4-Carboxybutyl)triphenylphosphonium bromide | HCID 161236 | — |
반응 단계
A mixture of 103 g. of 5-bromovaleric acid and 152 g. of triphenylphosphine in 400 ml. of acetonitrile is refluxed for 48 hours, cooled, diluted with 100 ml. of benzene and allowed to crystallize. The crystals are filtered, washed with benzene and ether, to yield colorless material, m.p. 207°-209° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04152524 |
| 출처 데이터셋 | uspto-grants-1979_05 |
| ORD ID | ord-ac6a772fb3ad443cbafbec131e02d7b2 |
| 출처 메모 | uspto-grants-1979_05 |