Ethylenediamine → HCID 178484974, 화합물

HRID 262672노트

반응식

HRID 262672 반응식
C(N)CN.ClCC1SC=CN=1.[S:12]1[CH:16]=[CH:15][N:14]=[C:13]1[CH2:17][NH:18][CH2:19][CH2:20][NH2:21].[C:22]([NH:24][C:25](=[N:28][CH3:29])SC)#[N:23]>>[C:22]([NH:24][C:25]([NH:28][CH3:29])=[N:21][CH2:20][CH2:19][NH:18][CH2:17][C:13]1[S:12][CH:16]=[CH:15][N:14]=1)#[N:23]

참가 물질

5

반응물 4

HCID 3301EthylenediamineHCID 1111031-Cyano-2,3-dimethylisothioureaHCID 140908642-(Chloromethyl)-1,3-thiazoleHCID 17944882N-(2-thiazolylmethyl)ethylenediamine

생성물 1

HCID 178484974HCID 178484974, 화합물

실험 절차

Reacting ethylenediamine with 2-chloromethylthiazole by the procedure of Example 34, then reacting the resulting N-(2-thiazolylmethyl)ethylenediamine with N-cyano-N',S-dimethylisothiourea by the procedure of Example 3(a), gives N-cyano-N'-methyl-N"-[2-(2-thiazolylmethylamino)ethyl]guanidine. Hydrolysis of this compound by the procedure of Example 3(e) gives N-methyl-N'-[2-(2-thiazolylmethylamino)ethyl]guanidine trihydrochloride.

출처 및 근거

ORD 기록
ord-98ab53dfa41e437e99687f6be6f28408
출처 데이터셋
uspto-grants-1979_05
특허 번호
US04154844

반응 노트

불러오는 중…