Ethylenediamine → N-(3-isothiazolylmethyl)ethylenediamine

HRID 262675노트

반응식

HRID 262675 반응식
[CH2:1]([NH2:4])[CH2:2][NH2:3].Br[CH2:6][C:7]1[CH:11]=[CH:10][S:9][N:8]=1>>[S:9]1[CH:10]=[CH:11][C:7]([CH2:6][NH:3][CH2:2][CH2:1][NH2:4])=[N:8]1

참가 물질

3

반응물 2

HCID 3301EthylenediamineHCID 130375983-(bromomethyl)Isothiazole

생성물 1

HCID 20557777N-(3-isothiazolylmethyl)ethylenediamine

실험 절차

By the procedure of Example 34, ethylenediamine is reacted with 3-bromomethylisothiazole to give N-(3-isothiazolylmethyl)ethylenediamine. This intermediate is heated under reflux with S-methylisothiouronium sulphate in water for 3 hours by the procedure of Example 1 to give the title compound.

출처 및 근거

ORD 기록
ord-147056502ddc49e292fff201955e376b
출처 데이터셋
uspto-grants-1979_05
특허 번호
US04154844

반응 노트

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