Anthracene → Potassium Anthracene

HRID 2636

반응식

HRID 2636 반응식
[CH:1]1[C:14]2[C:5](=[CH:6][C:7]3[C:12]([CH:13]=2)=[CH:11][CH:10]=[CH:9][CH:8]=3)[CH:4]=[CH:3][CH:2]=1.[K:15]>COCCOC>[CH:4]1[C:5]2[C:14](=[CH:13][C:12]3[C:7]([CH:6]=2)=[CH:8][CH:9]=[CH:10][CH:11]=3)[CH:1]=[CH:2][CH:3]=1.[K:15]

참가 물질

4

반응물 2

HCID 8418AnthraceneHCID 5462222Potassium

생성물 1

HCID 86741178Potassium Anthracene

시약·촉매·용매 1

HCID 80711,2-Dimethoxyethane용매

실험 절차

A potassium anthracene solution is prepared by adding about 17.8 gm of anthracene to about 500 ml of ethylene glycol dimethyl ether (monoglyme) in a flask in a glove box. A total of about 3.8 gm potassium metal is then added to the mixture. This composition gives a 5% by weight KAn solution. The mixture is then stirred overnight to allow the KAn formation to complete. The solution is then brought out of the glove box and placed into a large glass vessel blanketed with Ar gas. The bath effectiveness in modifying the surface of RO2800 samples was periodically tested. The experiment is terminated after 90 hours with the solution still being active.

후처리

  1. customThis composition gives a 5% by weight KAn solution
  2. customplaced into a large glass vessel
  3. customThe experiment is terminated after 90 hours with the solution

출처 및 근거

ORD 기록
ord-9c395594dc1e40538a243005b001547e
출처 데이터셋
uspto-grants-1998_03
특허 번호
US05730890

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