Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-[6-Fluoro-2-methyl-3-[(4-methylsulfonylphenyl)methylidene]inden-1-yl]acetic acid → Sodium 5-fluoro-2-methyl-1-(rho-methylsulfonylbenzylidene)-3-indenylacetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-[6-Fluoro-2-methyl-3-[(4-methylsulfonylphenyl)methylidene]inden-1-yl]acetic acid | HCID 114866 | — |
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Sodium 5-fluoro-2-methyl-1-(rho-methylsulfonylbenzylidene)-3-indenylacetate | HCID 70149782 | — |
반응 단계
5-fluoro-2-methyl-1-(ρ-methylsulfonylbenzylidene)-3-indenylacetic acid (1.79 g.) in methanol (10 ml.) is added to a solution of sodium methoxide (0.27 g.) in methanol (5 ml.). The reaction mixture is stirred for 20 minutes and evaporated to dryness to yield sodium 5-fluoro-2-methyl-1-(ρ-methylsulfonylbenzylidene)-3-indenylacetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05643959 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-cd04c875f5ec4961a8fe1d10a69de86b |
| 출처 메모 | uspto-grants-1997_07 |