2-Methylbutylamine → N-2-methylbutyl-4-acetamidobenzamide

HRID 263649

반응식

HRID 263649 반응식
[N+](C1C=C[C:7]([C:8](Cl)=[O:9])=CC=1)([O-])=O.CC(CC)CN.[CH3:19][CH:20]([CH2:34][CH3:35])[CH2:21][NH:22][C:23](=[O:33])[C:24]1[CH:29]=[CH:28][C:27]([N+:30]([O-])=O)=[CH:26][CH:25]=1>>[CH3:19][CH:20]([CH2:34][CH3:35])[CH2:21][NH:22][C:23](=[O:33])[C:24]1[CH:29]=[CH:28][C:27]([NH:30][C:8](=[O:9])[CH3:7])=[CH:26][CH:25]=1

참가 물질

4

반응물 3

HCID 72832-MethylbutylamineHCID 85024-Nitrobenzoyl chlorideHCID 9899490N-2-methylbutyl-4-nitrobenzamide

생성물 1

HCID 9813640N-2-methylbutyl-4-acetamidobenzamide

실험 절차

The method of Example 3 is repeated using 4-nitrobenzoyl chloride and 2-methylbutyl amine in the amidation step. This yields N-2-methylbutyl-4-nitrobenzamide (CPI1146).

출처 및 근거

ORD 기록
ord-a3b986df18684cb3902d1dcb4c77af71
출처 데이터셋
uspto-grants-1997_07
특허 번호
US05643965

연결된 노트

불러오는 중…